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Beilstein J. Org. Chem. 2017, 13, 728–733, doi:10.3762/bjoc.13.72
Graphical Abstract
Figure 1: The derivatives of all-cis-2,3,5,6-tetrafluorocyclohexane.
Scheme 1: Reagents and conditions: a) Li (2.5 equiv), NH3, t-BuOH (1 equiv), MeI (2 equiv), 3 h, −78 °C, 18 h...
Scheme 2: Reagents and conditions: a) Et3N·3HF (8 equiv), 18 h, 140 °C; b) Tf2O (4 equiv), pyridine, 1 h, 0 °...
Scheme 3: Reagents and conditions: a) Et3N·3HF (8 equiv), 18 h, 140 °C; b) Tf2O (4 equiv), pyridine, 1 h, 0 °...
Scheme 4: Reagents and conditions: a) terephthaloyl chloride (1 equiv), Et3N (4 equiv), DMAP (20 mol %), DCM,...
Figure 2: X-ray structures and crystal packing of compounds 13, 14 and 15.